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DIAS, R. R. ; CABANELLAS, D. ; KOTIK, H. G. ; CAMERINI, CESAR G. ; ZATTERA, A. ; PEREIRA, I. (2022).
Resumo: Ballistic helmets are individual pieces of armor equipment designed to protect a soldier’s head from projectiles and fragments. Although very common, these helmets are responsible for several casualties due to their significant back face deformation and low ballistic resistance to projectiles. Therefore, to enhance helmet performance, studies have focused on the development of new materials and new ballistic protection solutions. The purpose of this study was to develop and evaluate a new ballistic solution using thermoplastic-based matrices. The first matrix was based on high-density polyethylene (HDPE). The second matrix was based on HDPE modified with exfoliated montmorillonite (MMT). The main manufacturing processes of a thermoplastic-based ballistic helmet are presented, along with its ballistic performance, according to the National Institute of Justice (NIJ) standard 0106.01 and an investigation of its failure mechanisms via a non-destructive technique. All the helmets resulted in level III-A ballistic protection. The postimpact helmets were scanned to evaluate the back face deformation dimensions, which revealed that the global cone deformation was deeper in the HDPE than in the HDPE/MMT helmet. The failure analysis revealed an overall larger deformation area in the HDPE and HDPE/MMT helmet delamination zones in the regions with a large radius of curvature than in the zones with the lowest radius, which is in accordance with previous simulations reported in the literature.
BORBOREMA, SINARA ; DE HOLANDA FERRER, VITOR ; ROCHA, ADRIANA DA CUNHA ; COSSÚ, CAIO MARCELLO FELBINGER AZEVEDO ; NUNES, ALINE RAQUEL VIEIRA ; NUNES, CARLOS ANGELO ; MALET, LOIC ; DE ALMEIDA, LUIZ HENRIQUE. (2022).
Resumo: Metastable β-Ti alloys have become one of the most attractive implant materials due to their high biocorrosion resistance, biocompatibility, and mechanical properties, including lower Young’s modulus values. Mechanical properties of these alloys are strongly dependent on the final microstructure, which is controlled by thermomechanical treatment processing, in particular the Young’s modulus and hardness. The aim of this work was to analyze the influence of phase precipitations in heat-treated Ti-12Mo-xNb (x = 0, 3, 8, 13, 17, and 20) alloys. The alloys were prepared via arc melting and treated at 950 °C/1 h, and then quenched in water. The microstructures were analyzed by optical microscopy, transmission electron microscopy, and X-ray diffraction. Mechanical properties were based on Vickers microhardness tests and Young’s modulus measurements. Microstructural characterization showed that α″ and ω stability is a function of Nb content for the Ti–12Mo base alloy. Nb addition resulted in the suppression of the α″ phase and decrease in the ω phase volume fraction. Although the ω phase decreased with higher Nb contents, ω particles with ellipsoidal morphology were still observed in the Ti–12Mo–20Nb alloy. The α″ phase suppression by Nb addition caused a marked increase in the Young’s modulus, which decreased back to lower values with higher Nb concentrations. On other hand, the decrease in the ω phase continuously reduced alloy hardness. The study of the effect of chemical composition in controlling the volume fraction of these phases is an important step for the development of β-Ti alloys with functional properties.
MARTINS, A. L. B. S ; SILVA, E. F. ; MARQUES, M. F. V. ; PINHEIRO, W. A. (2022).
Resumo: The present work compares graphene oxides produced by the Marcano's method and the subsequent reduction process using a microwave system with different power and time sets. The thermal profiles of the reduction processes were analyzed, emphasizing the heat capacity from the 600 W test of 3.44 kJ/K. The X-ray diffraction showed a reduction in the interlayer space and the number of layers in all powers. The infrared and UV-Vis spectroscopy results showed a clear decrease in the bands corresponding to the oxygenated group and partial restoration of aromatic bonds. The Raman spectroscopy showed that the 1000 W power set originated a higher defective structure. The observed results allow the conclusion that the 600 W power promotes a little better result between the analyzed power sets.
